This article describes the preparation, characterization and Kinetics of bimetallic alloy nanoparticles of GO-Ni-Cu NPs. The main objective of this review is to quantitatively, and comprehensively describe the synthesis of bimetallic nanoparticles, and characterization. The kinetic studies were carried out as a function of different variables like pH, and temperature on rate of decolorization. The activation energy in presence of Go- Ni(II) and Go-Cu(II) is lower than in its Go-Ni-Cu. The reaction to be [H+] because the first order in both [MB+] and reductant. The rate was found to increase linearly with temperature. The rate of decolorization decreased after the addition of Ni(II), but increased after the addition of Cu(II). The decrease in the activation energy(Ea) in presence of these transition metal ions confirms their catalytic effects (metal activation). Cu–Ni BNP implant to the graphene oxide surface and it increases the catalytic activity and also dispersion capacity.