The Cadmium Sulfide Nanoparticles (CdS NPs) are drawn up using the green synthesis method. In the existing interpretation, Hibiscus rosa sinesis leaves extract is utilized as a natural stabilizer. Cadmium is obtained from sources being cadmium chloride, cadmium nitrate, cadmium sulphate, and sodium sulphide applied as a determinant of sulphur. In pursuance of determining the nature of a material, band gap, functional compounds, elemental analysis, as well as surface morphology of the synthesized material, the rehearsed CdSNPs prevail, being characterized by carrying out X-Ray Diffraction (XRD), UV-Visible Absorption spectroscopy, Fourier Transform Infrared (FTIR) spectroscopy, furthermore Scanning Electron Microscopy (SEM) experimental techniques. These tests have shown that the rehearsed materials were found as cubic crystalline cadmium sulphide with an average particle size of less than 10 nm. FTIR has demonstrated that a thin molecular layer has developed on the surface of the cadmium sulphide nanoparticles.